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DIMETHYL 2-(3'',3''-DIMETHYLBUTYL)MALONATE synthesis

4synthesis methods
-

Yield:153742-13-3 35%

Reaction Conditions:

with N,N,N,N,N,N-hexamethylphosphoric triamide;sodium hydride in tetrahydrofuran; for 16 h;Heating;

References:

Provencher;Wynn;Jones;Krawczyk [Tetrahedron Asymmetry,1993,vol. 4,# 9,p. 2025 - 2026]