ChemicalBook CAS DataBase List DiMethyl 5-ChloroMethyl-1,3-Benzene-Dicarboxylate

DiMethyl 5-ChloroMethyl-1,3-Benzene-Dicarboxylate synthesis

4synthesis methods

Product Name:DiMethyl 5-ChloroMethyl-1,3-Benzene-Dicarboxylate
CAS Number:252210-01-8
Molecular formula:C11H11ClO4
Molecular Weight:242.66

2672-58-4 Synthesis

2672-58-4
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$7.00/5g

DiMethyl 5-ChloroMethyl-1,3-Benzene-Dicarboxylate

252210-01-8
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: 76 percent / 0.1 M aq. NaOH / methanol / 18 h
2: 88 percent / borane-methyl sulfide / tetrahydrofuran / 24 h / 27 °C
3: 93 percent / SOCl₂ / 1 h / Heating

References:

Dimick, Sarah M.;Powell, Steven C.;McMahon, Stephen A.;Moothoo, Davina N.;Naismith, James H.;Toone, Eric J. [Journal of the American Chemical Society,1999,vol. 121,# 44,p. 10286 - 10296]

1,3-Benzenedicarboxylic acid, 5-(hydroxyMethyl)-, 1,3-diMethyl ester

109862-53-5
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252210-01-8
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References

1,3,5-BENZENETRICARBOXYLIC ACID DIMETHYL ESTER

38588-64-6
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$98.00/100mg

252210-01-8
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References

554-95-0 Synthesis

554-95-0
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$6.00/25g

252210-01-8
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References