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17165-18-3

Diphenylphosphinostyrene synthesis

5synthesis methods
-

Yield:17165-18-3 81%

Reaction Conditions:

Stage #1: Methyltriphenylphosphonium bromidewith sodium amide in tetrahydrofuran at 20; for 0.5 h;
Stage #2: (2-formylphenyl)(diphenyl)phosphine in tetrahydrofuran at 20; for 4 h;Wittig reaction;

References:

Williams, D. Bradley G.;Shaw, Megan L. [Tetrahedron,2007,vol. 63,# 7,p. 1624 - 1629]