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ChemicalBook CAS DataBase List DL-HoMocysteine Thiolactone--d4 HCl

DL-HoMocysteine Thiolactone--d4 HCl synthesis

1synthesis methods
-

Yield:1219805-31-8 91%

Reaction Conditions:

Stage #1: DL-[3,3,4,4-(2)H4]methioninewith hydrogen iodide in water; for 9 h;Reflux;
Stage #2: in water;

References:

Shinohara, Yoshihiko;Hasegawa, Hiroshi;Hashimoto, Takao;Ichida, Kimiyoshi [Journal of labelled compounds and radiopharmaceuticals,2010,vol. 53,# 8,p. 552 - 555] Location in patent:experimental part