Dodecanedioic acid, Mono(1,1-diMethylethyl) ester synthesis
- Product Name:Dodecanedioic acid, Mono(1,1-diMethylethyl) ester
- CAS Number:234081-98-2
- Molecular formula:C16H30O4
- Molecular Weight:286.41
693-23-2
424 suppliers
$5.00/25g
115-11-7
233 suppliers
$45.00/25 g
234081-98-2
85 suppliers
$17.00/100mg
Yield: 95.3%
Reaction Conditions:
with graphene-ferric oxide composite nanomaterial in dichloromethane for 4 h;Cooling with ice;Solvent;Reagent/catalyst;
Steps:
3-6; 11 Example 3
The solution of dodecyl diacid (1 mmol) and 1 mmol of isobutylene in isopropyl ether was dissolved in dichloromethane, and 5 mg of product A was added under ice salt bath. After stirring for 4 hours, the product A was recovered by magnetic separation. The reaction solution was concentrated to obtain mono-tert-butyl dodecyl dicarboxylate (273 mg, yield: 95.3%, purity: 90.5%).
References:
Yangzhou Industry Polytechnic College;Chen Kequan;Luo Zhichen;Yue Jinfang;Wang Xueyuan;Du Bin;Yin Fan CN109111361, 2019, A Location in patent:Paragraph 0037-0046; 0059-0060
693-23-2
424 suppliers
$5.00/25g
75-65-0
743 suppliers
$10.00/10ml
234081-98-2
85 suppliers
$17.00/100mg