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ChemicalBook CAS DataBase List DPO-1
43077-30-1

DPO-1 synthesis

10synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: sodium / tetrahydrofuran; mineral oil / 1 h / 25 °C / Inert atmosphere
2: N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran / 16 h / 25 - 67 °C

References:

Ye, Jingjing;Zhang, Jian-Qiu;Saga, Yuta;Onozawa, Shunya;Kobayashi, Shu;Sato, Kazuhiko;Fukaya, Norihisa;Han, Li-Biao [Organometallics,2020,vol. 39,# 14,p. 2682 - 2694]

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