ChemicalBook CAS DataBase List (E)-4-phenylbut-3-en-1-amine

(E)-4-phenylbut-3-en-1-amine synthesis

3synthesis methods

Product Name:(E)-4-phenylbut-3-en-1-amine
CAS Number:82593-25-7
Molecular formula:C10H13N
Molecular Weight:147.22

591-50-4 Synthesis

591-50-4
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82593-25-7
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Yield:-

Steps:

Multi-step reaction with 4 steps
1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 10 h / 20 °C / Inert atmosphere; Glovebox; Schlenk technique
2: lithium aluminium tetrahydride / 3 h / 0 - 20 °C / Inert atmosphere; Glovebox; Schlenk technique
3: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 3 h / 0 °C / Inert atmosphere; Glovebox
4: hydrazine hydrate / ethanol / 1 h / 50 °C / Inert atmosphere; Glovebox

References:

Zhao, Lei;Meng, Xiao;Zou, Yifeng;Zhao, Junsong;Wang, Lili;Zhang, Lanlan;Wang, Chao [Organic Letters,2021,vol. 23,# 21,p. 8516 - 8521]

1H-Isoindole-1,3(2H)-dione, 2-(4-phenyl-3-buten-1-yl)-

143741-67-7
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82593-25-7
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References

10229-11-5 Synthesis

10229-11-5
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82593-25-7
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References