(E)-Caffeic Acid Diacetate synthesis
- Product Name:(E)-Caffeic Acid Diacetate
- CAS Number:88623-81-8
- Molecular formula:C13H12O6
- Molecular Weight:264.23
331-39-5
675 suppliers
$5.00/100mg
108-24-7
5 suppliers
$14.00/250ML
88623-81-8
19 suppliers
$165.00/500mg
Yield:88623-81-8 100%
Reaction Conditions:
with pyridine at 20;
Steps:
2.5 Syntheses of coumarate and caffeate derivatives
A solution of caffeic acid (180 mg, 1.0 mmol) in dry pyridine (0.3 mL) was added of acetic anhydride (0.47 mL, 5 mmol) and then stirred at r.t. over night.
The reaction mixture was gently heated under vacuum to evaporate excess acetic anhydride and pyridine thus obtaining quantitatively (2E)-3-[3,4-bis(acetyloxy)phenyl]-2-propenoic acid (264 mg, 1.0 mmol).
References:
D'Ambrosio, Michele [Food Chemistry,2013,vol. 138,# 4,p. 2079 - 2088]
331-39-5
675 suppliers
$5.00/100mg
88623-81-8
19 suppliers
$165.00/500mg
331-39-5
675 suppliers
$5.00/100mg
108-24-7
5 suppliers
$14.00/250ML
88623-81-8
19 suppliers
$165.00/500mg
867-13-0
462 suppliers
$10.00/1g
67727-64-4
41 suppliers
$19.05/Price $/250mgs:
88623-81-8
19 suppliers
$165.00/500mg
108-24-7
5 suppliers
$14.00/250ML
139-85-5
815 suppliers
$5.00/1g
88623-81-8
19 suppliers
$165.00/500mg