(E)-N-[1-(4-nitrophenyl)ethylidene]hydroxylamine synthesis
- Product Name:(E)-N-[1-(4-nitrophenyl)ethylidene]hydroxylamine
- CAS Number:59862-56-5
- Molecular formula:C8H8N2O3
- Molecular Weight:180.16
100-19-6
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Yield:59862-56-5 100%
Reaction Conditions:
with hydroxylamine hydrochloride;sodium acetate in methanol;water;Reflux;
Steps:
19.
All of the oxime substrates used in this investigation were synthesized in quantitative yields by refluxing a mixture of 1 equiv of the corresponding ketones or aldehydes, 1.6 equiv of hydroxylamine hydrochloride, and 2.0 equiv of sodium acetate in aqueous methanol.
References:
Augustine, John Kallikat;Kumar, Rajesha;Bombrun, Agnes;Mandal, Ashis Baran [Tetrahedron Letters,2011,vol. 52,# 10,p. 1074 - 1077] Location in patent:experimental part
100-13-0
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