ChemicalBook CAS DataBase List EHT 5372

EHT 5372 synthesis

6synthesis methods

Product Name:EHT 5372
CAS Number:1425945-60-3
Molecular formula:C18H14FN5O2S
Molecular Weight:383.4

17420-30-3 Synthesis

17420-30-3
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$7.00/25g

1425945-60-3
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Yield:-

Steps:

Multi-step reaction with 9 steps
1: triethylamine; dmap / dichloromethane / 4 h / 20 °C / Inert atmosphere
2: palladium on activated charcoal; ammonium formate / ethanol / 0.5 h / 85 °C / Inert atmosphere; Microwave irradiation
3: bromine; acetic acid / dichloromethane / 2.5 h / 20 °C / Inert atmosphere
4: pyridine / dichloromethane / 4 h / 20 °C / Inert atmosphere
5: acetic acid / 2 h / 118 °C / Inert atmosphere; Microwave irradiation
6: copper(l) iodide / pyridine / 0.33 h / 130 °C / Inert atmosphere; Microwave irradiation
7: N,N-dimethyl-formamide / 0.03 h / 70 °C / Inert atmosphere; Microwave irradiation
8: acetic acid / 0.83 h / 118 °C / Inert atmosphere; Microwave irradiation
9: methanol / 0.5 h / 65 °C / Inert atmosphere; Microwave irradiation

References:

Chaikuad, Apirat;Diharce, Julien;Schröder, Martin;Foucourt, Alicia;Leblond, Bertrand;Casagrande, Anne-Sophie;Désiré, Laurent;Bonnet, Pascal;Knapp, Stefan;Besson, Thierry [Journal of Medicinal Chemistry,2016,vol. 59,# 22,p. 10315 - 10321]

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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124-41-4 Synthesis

124-41-4
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$12.00/25g

1425945-60-3
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References

Carbamic acid, N-(4-amino-3-bromo-2-cyanophenyl)-, 1,1-dimethylethyl ester

1425945-82-9
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1425945-60-3
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References

tert-butyl 2-cyano-4-nitrophenylcarbamate

1425945-81-8
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1425945-60-3
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References

Carbamic acid, N-(4-amino-2-cyanophenyl)-, 1,1-dimethylethyl ester

1156096-32-0
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1425945-60-3
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References