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Estra-1,3,5(10)-trien-17-one, 3-iodo- synthesis

3synthesis methods
Estra-1,3,5(10)-trien-17-one, 3-[[(trifluoromethyl)sulfonyl]oxy]-

92817-04-4
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Estra-1,3,5(10)-trien-17-one, 3-iodo-

1243197-32-1
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Yield:1243197-32-1 58%

Reaction Conditions:

with iodine;lithium fluoride;sodium iodide in acetonitrile at 25; for 24 h;Inert atmosphere;UV-irradiation;Schlenk technique;

References:

Liu, Wenbo;Yang, Xiaobo;Gao, Yang;Li, Chao-Jun [Journal of the American Chemical Society,2017,vol. 139,# 25,p. 8621 - 8627] Location in patent:supporting information