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ChemicalBook CAS DataBase List EthaniMidaMide, N,N'-bis(1-Methylethyl)-

EthaniMidaMide, N,N'-bis(1-Methylethyl)- synthesis

3synthesis methods
-

Yield: 80%

Reaction Conditions:

Stage #1:Trimethyl orthoacetate;isopropylamine with acetic acid for 12 h;Heating / reflux;
Stage #2: with sodium methylate in methanol;n-heptane at 20; for 1 h;

References:

TOSOH CORPORATION;SAGAMI CHEMICAL RESEARCH CENTER WO2007/15436, 2007, A1 Location in patent:Page/Page column 11