Ethanone, 1-(2-methyl-6-benzothiazolyl)- (9CI) synthesis

6synthesis methods

Product Name:Ethanone, 1-(2-methyl-6-benzothiazolyl)- (9CI)
CAS Number:20077-92-3
Molecular formula:C10H9NOS
Molecular Weight:191.25

1030373-71-7 Synthesis

1030373-71-7
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Ethanone, 1-(2-methyl-6-benzothiazolyl)- (9CI)

20077-92-3
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Yield:20077-92-3 71%

Reaction Conditions:

Stage #1: N-(4-acetyl-2-iodophenyl)acetamidewith copper(l) iodide;potassium sulfide in N,N-dimethyl-formamide at 80; for 12 h;
Stage #2: with hydrogenchloride in N,N-dimethyl-formamide at 20;

References:

Ma, Dawei;Xue, Peng;Jiang, Yongwen;Xie, Siwei;Zhang, Xiaojing;Dong, Jinhua [Angewandte Chemie - International Edition,2009,vol. 48,# 23,p. 4222 - 4225] Location in patent:supporting information; experimental part

101209-08-9
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$57.00/5g

20077-92-3
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20077-92-3
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103440-65-9
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$119.00/100mg

20077-92-3
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6-Benzothiazolecarboxaldehyde,2-methyl-(8CI,9CI)

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20077-92-3
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References