ChemicalBook CAS DataBase List Ethanone, 1-(4-amino-3-methylphenyl)- (9CI)

Ethanone, 1-(4-amino-3-methylphenyl)- (9CI) synthesis

9synthesis methods

Product Name:Ethanone, 1-(4-amino-3-methylphenyl)- (9CI)
CAS Number:43230-11-1
Molecular formula:C9H11NO
Molecular Weight:149.19

96784-58-6
9 suppliers
inquiry

Ethanone, 1-(4-amino-3-methylphenyl)- (9CI)

43230-11-1
9 suppliers
inquiry

Yield:43230-11-1 98 %Chromat.

Reaction Conditions:

with hydrogen in toluene at 120; under 11251.1 Torr;Autoclave;

Steps:

2.3. Catalytic performance test and procedure for recycling test

General procedure: Catalytic Performance Test. A mixture of nitroarenes (1.0 mmol),catalyst (80 mg, 3.8 wt%) were added to a glass tube which was placed in a 100 mL autoclave. Then the autoclave was purged and charged with H2 (1.5 MPa) three times. The reaction mixture was stirred at 120 °C for 12 h. Then, the autoclave was cooled to room temperature and the pressure was carefully released. Subsequently, the reaction mixture was diluted with 10 mL toluene for quantitative analysis by GC-FID (Agilent 7890B-5977A).

References:

Dai, Xingchao;He, Dongcheng;Li, Teng;Shi, Feng;Wang, Hongli;Wang, Tao;Wang, Xinzhi [Journal of Catalysis,2021,vol. 400,p. 397 - 406]