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ChemicalBook CAS DataBase List ETHANONE, 1-(5-BROMO-2,4-DIMETHOXYPHENYL)

ETHANONE, 1-(5-BROMO-2,4-DIMETHOXYPHENYL) synthesis

2synthesis methods
Obtained by reaction of acetic anhydride with 1-bromo-2,4-dimethoxybenzene in the presence of boron trifluoride etherate in methylene chloride first at 0°, then at r.t. for 24 h (85%).
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Yield:182056-48-0 99%

Reaction Conditions:

with bromine;acetic acid at -20; for 0.716667 h;

References:

Mihigo, Shetonde O.;Mammo, Wendimagegn;Bezabih, Merhatibeb;Andrae-Marobela, Kerstin;Abegaz, Berhanu M. [Bioorganic and Medicinal Chemistry,2010,vol. 18,# 7,p. 2464 - 2473] Location in patent:scheme or table

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