Ethanone, 1-(5-nitro-3-isoxazolyl)- (9CI) synthesis
- Product Name:Ethanone, 1-(5-nitro-3-isoxazolyl)- (9CI)
- CAS Number:340014-77-9
- Molecular formula:C5H4N2O4
- Molecular Weight:156.0963
Yield:340014-77-9 80%
Reaction Conditions:
Stage #1: tetranitromethanewith triethylamine in 1,4-dioxane at 0; for 0.0833333 h;Inert atmosphere;
Stage #2: methyl vinyl ketone in 1,4-dioxane at 20; for 12 h;Inert atmosphere;Reagent/catalyst;Solvent;
References:
Volkova, Yulia A.;Averina, Elena B.;Vasilenko, Dmitry A.;Sedenkova, Kseniya N.;Grishin, Yuri K.;Bruheim, Per;Kuznetsova, Tamara S.;Zefirov, Nikolai S. [Journal of Organic Chemistry,2019,vol. 84,# 6,p. 3192 - 3200] Location in patent:supporting information
5029-48-1
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