Ethanone, 1-cyclohexyl-2-(2-piperidinyl)- synthesis
- Product Name:Ethanone, 1-cyclohexyl-2-(2-piperidinyl)-
- CAS Number:1083048-37-6
- Molecular formula:C13H23NO
- Molecular Weight:209.33
110-89-4
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: n-butyllithium / diethyl ether; hexane / 0.08 h / -78 °C / Inert atmosphere
1.2: 0.08 h / -78 °C / Inert atmosphere
2.1: trifluoroacetic acid / diethyl ether; hexane; tetrahydrofuran / 0.08 h / -78 °C / Inert atmosphere
2.2: 2 h / -78 - 20 °C / Inert atmosphere
References:
Paul, Anirudra;Kim, Jae Hyun;Daniel, Scott D.;Seidel, Daniel [Angewandte Chemie - International Edition,2021,vol. 60,# 3,p. 1625 - 1628][Angew. Chem.,2021,vol. 133,# 3,p. 1649 - 1652,4]
