Ethanone, 2-diazo-1-(3-methylphenyl)- synthesis

4synthesis methods

Product Name:Ethanone, 2-diazo-1-(3-methylphenyl)-
CAS Number:7023-80-5
Molecular formula:C9H8N2O
Molecular Weight:160.1726

585-74-0 Synthesis

585-74-0
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Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: NBS; toluene-4-sulfonic acid / acetonitrile / 25 °C / Reflux
2.1: 4-methyl-N'-(p-tolylsulfonyl)benzenesulfonohydrazide / tetrahydrofuran / 0.08 h / 0 °C
2.2: 0.5 h / 0 °C

References:

Chen, Hong-Ru;Qin, Hua-Li;Shu, Tao;Tang, Haolin;Yang, Wen-Fei [Organic and Biomolecular Chemistry,2022,vol. 20,# 17,p. 3506 - 3510]

1,3-bis(3-methylphenyl)propane-1,3-dione

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References

51012-64-7 Synthesis

51012-64-7
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$139.00/1g

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99-04-7 Synthesis

99-04-7
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References