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ChemicalBook CAS DataBase List Ethyl 2-cyclohexyl-2-oxoacetate

Ethyl 2-cyclohexyl-2-oxoacetate synthesis

14synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: magnesium; iodine / tetrahydrofuran / 2 h / 55 - 60 °C / Large scale
2: tetrahydrofuran / 3 h / -40 - -5 °C / Inert atmosphere; Large scale

References:

ASYMCHEM LABORATORIES (TIANJIN) CO., LTD;ASYMCHEM LIFE SCIENCE (TIANJIN) CO., LTD;TIANJIN ASYMCHEM PHARMACEUTICAL CO., LTD;ASYMCHEM LABORATORIES (FUXIN) CO., LTD;JILIN ASYMCHEM LABORATORIES CO., LTD.;Hong, Hao;Zheng, Changsheng;Guo, Lina US2016/319312, 2016, A1

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