ETHYL 2-METHOXY-1-NAPHTHOYLFORMATE synthesis
- Product Name:ETHYL 2-METHOXY-1-NAPHTHOYLFORMATE
- CAS Number:22531-51-7
- Molecular formula:C15H14O4
- Molecular Weight:258.27
17075-39-7
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$305.00/1g
4755-77-5
343 suppliers
$9.00/25g
22531-51-7
15 suppliers
$251.00/1g
Yield:22531-51-7 80%
Reaction Conditions:
Stage #1: 4-chloro-1-methyl-naphthalenewith lithium in diethyl ether at 20; for 3 h;
Stage #2: with copper(l) cyanide in tetrahydrofuran;diethyl ether; for 0.25 h;Cooling with ice;
Stage #3: Ethyl oxalyl chloride in tetrahydrofuran;diethyl ether; for 0.666667 h;Cooling with ice;
References:
Screttas, Constantinos G.;Steele, Barry R.;Micha-Screttas, Maria;Heropoulos, Georgios A. [Organic Letters,2012,vol. 14,# 22,p. 5680 - 5683] Location in patent:supporting information
93-04-9
468 suppliers
$13.00/25g
4755-77-5
343 suppliers
$9.00/25g
22531-51-7
15 suppliers
$251.00/1g
7446-70-0
704 suppliers
$15.00/25g
93-04-9
468 suppliers
$13.00/25g
4755-77-5
343 suppliers
$9.00/25g
22531-51-7
15 suppliers
$251.00/1g