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ChemicalBook CAS DataBase List ethyl 3-(3-oxopropyl)benzoate

ethyl 3-(3-oxopropyl)benzoate synthesis

4synthesis methods
58313-23-8 Synthesis
ETHYL 3-IODOBENZOATE

58313-23-8
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ethyl 3-(3-oxopropyl)benzoate

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Yield:-

Steps:

Multi-step reaction with 3 steps
1: 92 percent / (PH3P)2PdCl2, CuI, Et2NH / 1.5 h / Ambient temperature
2: 91 percent / H2 / 5percent Pd/C / ethanol / 3 h / 760 Torr
3: 55 percent / pyridinium chlorochromate / CH2Cl2 / 4 h / Ambient temperature

References:

Chuang, Che-Ping;Gallucci, Judith C.;Hart, David J. [Journal of Organic Chemistry,1988,vol. 53,# 14,p. 3210 - 3218]