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Ethyl 3-(4-Chloro-2-nitrophenyl)propanoate synthesis

1synthesis methods
938-71-6 Synthesis
4-CHLORO-2-NITROBENZYL CHLORIDE

938-71-6
24 suppliers
$79.20/2g

105-36-2 Synthesis
Ethyl bromoacetate

105-36-2
348 suppliers
$5.00/5G

Ethyl 3-(4-Chloro-2-nitrophenyl)propanoate

1185180-58-8
8 suppliers
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Yield:1185180-58-8 23%

Reaction Conditions:

with Tetrakis(dimethylamino)ethylen in N,N-dimethyl-formamide at -20 - 70; for 3 h;Inert atmosphere;

References:

Since, Marc;Terme, Thierry;Vanelle, Patrice [Tetrahedron,2009,vol. 65,# 31,p. 6128 - 6134] Location in patent:experimental part