Ethyl (3,4-Dimethoxyphenyl)-difluoroacetate synthesis
- Product Name:Ethyl (3,4-Dimethoxyphenyl)-difluoroacetate
- CAS Number:125575-35-1
- Molecular formula:C12H14F2O4
- Molecular Weight:260.23
Yield:125575-35-1 68%
Reaction Conditions:
with copper(I) oxide;3,4,7,8-Tetramethyl-o-phenanthrolin;potassium carbonate in N,N-dimethyl-formamide at 80; for 16 h;Sealed tube;regioselective reaction;Friedel-Crafts Alkylation;
References:
Belhomme, Marie-Charlotte;Bayle, Alexandre;Poisson, Thomas;Pannecoucke, Xavier [European Journal of Organic Chemistry,2015,vol. 2015,# 8,p. 1719 - 1726] Location in patent:supporting information
93-40-3
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