ETHYL 4-(3-NITROPHENYL)-2,4-DIOXOBUTANOATE synthesis
- Product Name:ETHYL 4-(3-NITROPHENYL)-2,4-DIOXOBUTANOATE
- CAS Number:57961-49-6
- Molecular formula:C12H11NO6
- Molecular Weight:265.22
Yield:57961-49-6 87%
Reaction Conditions:
Stage #1: oxalic acid diethyl esterwith sodium methylate in diethyl ether at 20;Inert atmosphere;
Stage #2: 3-Nitroacetophenone in diethyl ether at 20; for 12 h;
References:
Nagarapu, Lingaiah;Gaikwad, Hanmant K.;Sarikonda, Kartheeka;Mateti, Jhansi;Bantu, Rajashaker;Raghu;Manda, Krishna Madhuri;Kalvendi, Shasi Vardhan [European Journal of Medicinal Chemistry,2010,vol. 45,# 11,p. 4720 - 4725] Location in patent:experimental part
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