ethyl 4-[(methoxycarbonyl)amino]benzoate synthesis
- Product Name:ethyl 4-[(methoxycarbonyl)amino]benzoate
- CAS Number:187741-67-9
- Molecular formula:C11H13NO4
- Molecular Weight:223.23
67-56-1
739 suppliers
$9.00/25ml
79-37-8
464 suppliers
$17.67/10gm:
94-09-7
765 suppliers
$5.00/50mg
187741-67-9
10 suppliers
$120.00/0.500g
Yield:187741-67-9 86%
Reaction Conditions:
Stage #1: oxalyl dichloride;p-aminoethylbenzoatewith hydrogenchloride in 1,4-dioxane;ethyl acetate at 5 - 10;
Stage #2: in 1,4-dioxane;1,2-dichloro-benzene at 130; for 3 h;
Stage #3: methanol in 1,4-dioxane;1,2-dichloro-benzene at 20 - 30;Further stages.;
References:
Oh, Lynette M.;Spoors, P. Grant;Goodman, Richard M. [Tetrahedron Letters,2004,vol. 45,# 24,p. 4769 - 4771]
6294-89-9
327 suppliers
$6.00/25g
94-09-7
765 suppliers
$5.00/50mg
187741-67-9
10 suppliers
$120.00/0.500g
67-56-1
739 suppliers
$9.00/25ml
201230-82-2
1 suppliers
inquiry
99-77-4
210 suppliers
$12.00/1mg
187741-67-9
10 suppliers
$120.00/0.500g
94-09-7
765 suppliers
$5.00/50mg
79-22-1
2 suppliers
$38.00/1000g
94-09-7
765 suppliers
$5.00/50mg
187741-67-9
10 suppliers
$120.00/0.500g
67-56-1
739 suppliers
$9.00/25ml
30806-83-8
55 suppliers
$60.00/50mg
187741-67-9
10 suppliers
$120.00/0.500g