ETHYL 5,5-DIMETHYL-4-OXOHEXANOATE synthesis

7synthesis methods

Product Name:ETHYL 5,5-DIMETHYL-4-OXOHEXANOATE
CAS Number:37174-98-4
Molecular formula:C10H18O3
Molecular Weight:186.25

75-11-6
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17094-34-7 Synthesis

17094-34-7
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37174-98-4
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$366.00/1g

Yield:37174-98-4 96%

Reaction Conditions:

Stage #1: diiodomethanewith diethylzinc;trifluoroacetic acid in dichloromethane; for 0.5 h;
Stage #2: ethyl pivaloylacetate in dichloromethane at 20; for 7 h;

References:

Xue, Song;Liu, Yong-Kang;Li, Le-Zhen;Guo, Qing-Xiang [Journal of Organic Chemistry,2005,vol. 70,# 20,p. 8245 - 8247]

3-Hexenoic acid, 5,5-dimethyl-4-(phenylthio)-, ethyl ester, (Z)- (9CI)

115205-55-5
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37174-98-4
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References

102690-35-7
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37174-98-4
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2-Butanol, 1-methoxy-3,3-dimethyl-1-(phenylthio)-

115205-35-1
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37174-98-4
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Propanedioic acid, 2-(3,3-dimethyl-2-oxobutylidene)-, 1,3-diethyl ester

854838-70-3
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37174-98-4
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Propanedioic acid, 2-(3,3-dimethyl-2-oxobutyl)-, 1,3-diethyl ester

85157-07-9
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References