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ChemicalBook CAS DataBase List Ethyl BroMoacetate-1,2-13C2

Ethyl BroMoacetate-1,2-13C2 synthesis

2synthesis methods
-

Yield:61898-49-5 93%

Reaction Conditions:

Stage #1:bromo[1,2-13C2]acetic acid with oxalyl dichloride at 20; for 30 h;
Stage #2:ethanol at 20; for 0.5 h;Further stages.;

References:

Creemers, Alain F. L.;Lugtenburg, Johan [Journal of the American Chemical Society,2002,vol. 124,# 22,p. 6324 - 6334]

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