Ethyl fluoroacetate synthesis
- Product Name:Ethyl fluoroacetate
- CAS Number:4792-10-3
- Molecular formula:C21H26N2O6
- Molecular Weight:402.44
809-27-8
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Yield:4792-10-3 87%
Reaction Conditions:
Stage #1: 4,4'-bis-(2-methoxycarbonyl-ethyl)-3,3'-dimethyl-5,5'-methanediyl-bis-pyrrole-2-carboxylic acidwith trifluoroacetic acid at 0; for 1.16667 h;Inert atmosphere;
Stage #2: with trimethyl orthoformate at 0 - 5;Inert atmosphere;
References:
Martin, Pierre;Mueller, Markus;Flubacher, Dietmar;Boudier, Andreas;Blaser, Hans-Ulrich;Spielvogel, Dirk [Organic Process Research and Development,2010,vol. 14,# 4,p. 799 - 804] Location in patent:experimental part