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Ethyl furo[3,2-b]pyridine-5-carboxylate synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1: 97 percent / m-chloroperbenzoic acid / CH2Cl2 / 20 h / Ambient temperature
2: 45 percent / triethylamine, benzoyl chloride / CH2Cl2 / 20 h / Ambient temperature
3: 78 percent / sodium ethoxide / 5 h / Ambient temperature
4: 97 percent / 10percent hydrochloric acid / ethanol; H2O / 14 h / Ambient temperature

References:

Shiotani, Shunsaku;Taniguchi, Katsunori [Journal of Heterocyclic Chemistry,1996,vol. 33,# 4,p. 1051 - 1056]