ETHYL TRANS-4-DECENOATE synthesis
- Product Name:ETHYL TRANS-4-DECENOATE
- CAS Number:76649-16-6
- Molecular formula:C12H22O2
- Molecular Weight:198.3
3391-86-4
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76649-16-6
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Yield:76649-16-6 99.9%
Reaction Conditions:
with propionic acid at 150; for 3 h;Claisen Rearrangement;Temperature;
Steps:
2.1 (1) Preparation of ethyl 4-decenoate
12.82 g of 1-octen-3-ol and 64.90 g of triethyl orthoacetate,Propionic acid 0.44g,Heated to 150 ,While distilling off the generated ethanol,The reaction was completed for about 3 hours.Excess distilled triethyl orthoacetate was distilled off under reduced pressure.Then use the oil pump distillation to get liquidEthyl 4-decenoate19.86g,Yield 99.9%.
References:
Beijing Liyuan Xin Sai Chemical Co., Ltd.;Jia Yanyong CN106748641, 2017, A Location in patent:Paragraph 0021; 0023; 0025
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3391-86-4
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$10.00/1g
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78-39-7
341 suppliers
$9.00/1g
76649-16-6
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$32.00/10mL
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1968-40-7
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74-85-1
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$79.00/11l
76649-16-6
78 suppliers
$32.00/10mL
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592-76-7
113 suppliers
$25.10/u
1968-40-7
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$27.89/1g
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76649-16-6
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$32.00/10mL
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