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Ethylenebis[bis(4-pyridyl)phosphine] synthesis

1synthesis methods
1120-87-2 Synthesis
4-Bromopyridine

1120-87-2
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Ethylenebis[bis(4-pyridyl)phosphine]

106323-58-4
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Yield:106323-58-4 91%

Reaction Conditions:

with n-butyllithium;N,N,N,N,-tetramethylethylenediamine at -115 - -80; for 2 h;

References:

Bowen, Richard J.;Garner, A. Christopher;Berners-Price, Susan J.;Jenkins, Ian D.;Sue, Rodney E. [Journal of Organometallic Chemistry,1998,vol. 554,# 2,p. 181 - 184]