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ethyltrimethylplumbane synthesis

4synthesis methods
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Yield:132125-74-7 89%

Reaction Conditions:

in tetrahydrofuran;byproducts: KCl; (Ar); added rapidly a soln. of B-compound to soln. of Pb-compound; refluxed for 5 h; filtered; evapd. (vac.); distd. (vac.); GC; elem. anal.;

References:

Koester, Roland;Seidel, Guenter;Wrackmeyer, Bernd [Chemische Berichte,1991,vol. 124,# 5,p. 1003 - 1016]