Fallacinol synthesis

14synthesis methods

Product Name:Fallacinol
CAS Number:569-05-1
Molecular formula:C16H12O6
Molecular Weight:300.26

90064-48-5 Synthesis

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Yield:-

Steps:

Multi-step reaction with 9 steps
1: 65 percent / NaH / EtOH / toluene / 1 h / Ambient temperature
2: 70 percent / NaOAc / 3 h / 140 °C
3: 78 percent / LiAlH₄ / tetrahydrofuran / 24 h / Ambient temperature
4: 90 percent / Et₃N, DMAP / CH₂Cl₂ / 5 h / Ambient temperature
5: 90 percent / cerium(IV) ammonium nitrate / acetonitrile; H₂O / 3 h / Ambient temperature
6: 84 percent / AlCl₃ / CH₂Cl₂ / 1 h / Ambient temperature
7: 75 percent / 1 h / 100 °C
8: 95 percent / AlCl₃ / CH₂Cl₂ / 24 h / Ambient temperature
9: 98 percent / 10percent aq. NaOH / 24 h / Ambient temperature

References:

Bloomer, James L.;Stagliano, Kenneth W.;Gazzillo, Joseph A. [Journal of Organic Chemistry,1993,vol. 58,# 27,p. 7906 - 7912]

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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569-05-1
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References

1000210-73-0
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569-05-1
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References

2100-42-7
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569-05-1
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References

9,10-Anthracenedione, 1,8-bis(acetyloxy)-3-methoxy-6-methyl-

25466-76-6
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569-05-1
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References