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ChemicalBook CAS DataBase List FEMA 2869

FEMA 2869 synthesis

4synthesis methods
By esterification of phenethyl alcohol with 3-methylcrotonic acid.
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Yield:42078-65-9 76%

Reaction Conditions:

with caesium carbonate;1-(tert-butylperoxy)-1,2-benziodoxol-3(1H)-one in cyclohexane at 25; for 46 h;

References:

Ochiai, Masahito;Ito, Takao;Takahashi, Hideo;Nakanishi, Akinobu;Toyonari, Mika;Sueda, Takuya;Goto, Satoru;Shiro, Motoo [Journal of the American Chemical Society,1996,vol. 118,# 33,p. 7716 - 7730]