FMOC-GLU(OBUT)-NH2 synthesis
- Product Name:FMOC-GLU(OBUT)-NH2
- CAS Number:104090-92-8
- Molecular formula:C24H28N2O5
- Molecular Weight:424.49
71989-18-9
433 suppliers
$7.00/5g
104090-92-8
24 suppliers
$40.00/1G
Yield:104090-92-8 99%
Reaction Conditions:
Stage #1: Fmoc-Glu(OtBu)-OHwith (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate;N-ethyl-N,N-diisopropylamine in dichloromethane at 20; for 0.333333 h;
Stage #2: with ammonia in dichloromethane;water; for 1.5 h;Further stages.;
References:
Singh, Yogendra;Stoermer, Martin J.;Lucke, Andrew J.;Glenn, Matthew P.;Fairlie, David P. [Organic Letters,2002,vol. 4,# 20,p. 3367 - 3370]