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71952-99-3

Fmoc-Gly-DL-Ala synthesis

3synthesis methods
29022-11-5 Synthesis
Fmoc-Gly-OH

29022-11-5
506 suppliers
$5.00/1g

Fmoc-Gly-DL-Ala

71952-99-3
2 suppliers
inquiry

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Yield:-

Steps:

Multi-step reaction with 3 steps
1: thionyl chloride / dichloromethane / 20 °C / Inert atmosphere; Sonication
2: zinc / tetrahydrofuran / 20 °C
3: water; calcium chloride; sodium hydroxide / isopropyl alcohol

References:

Ramesh;Raju;Srinivas;Sureshbabu;Vishwanatha;Hemantha [Rapid Communications in Mass Spectrometry,2011,vol. 25,# 14,p. 1949 - 1958]