ChemicalBook CAS DataBase List Fmoc-Ser(O-propargyl)-OH

Fmoc-Ser(O-propargyl)-OH synthesis

4synthesis methods

Product Name:Fmoc-Ser(O-propargyl)-OH
CAS Number:1354752-75-2
Molecular formula:C21H19NO5
Molecular Weight:365.38

82911-69-1 Synthesis

N-(9-Fluorenylmethoxycarbonyloxy)succinimide

82911-69-1
613 suppliers
$7.00/25g

(S)-2-tert-Butoxycarbonylamino-3-prop-2-ynyloxy-propionic acid

145205-94-3
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1354752-75-2
37 suppliers
$72.79/250MG

Yield:1354752-75-2 74%

Reaction Conditions:

Stage #1: (S)-2-[(tert-butoxycarbonyl)amino]-3-(prop-2-yn-1-yloxy)propanoic acidwith trifluoroacetic acid at 0; for 1 h;Inert atmosphere;
Stage #2: N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimidewith potassium carbonate in 1,4-dioxane;water at 0 - 20; for 3.5 h;Inert atmosphere;

References:

Sminia, Tjerk Jacco;Pedersen, Daniel Sejer [Synlett,2012,vol. 23,# 18,p. 2643 - 2646,4] Location in patent:supporting information Sminia, Tjerk Jacco;Pedersen, Daniel Sejer [Synlett,2012,vol. 23,# 18,p. 2643 - 2646] Location in patent:supporting information

145205-94-3
6 suppliers
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1354752-75-2
37 suppliers
$72.79/250MG

References

1379150-93-2
2 suppliers
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82911-69-1 Synthesis

82911-69-1
613 suppliers
$7.00/25g

1354752-75-2
37 suppliers
$72.79/250MG

References

L-Serine, N-[(1,1-dimethylethoxy)carbonyl]-O-2-propyn-1-yl-, methyl ester

675585-14-5
0 suppliers
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1354752-75-2
37 suppliers
$72.79/250MG

References