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ChemicalBook CAS DataBase List Formyl acetate

Formyl acetate synthesis

9synthesis methods
-

Yield:2258-42-6 100%

Reaction Conditions:

at 60; for 1 h;Inert atmosphere;

Steps:

17.1
Under the protection of nitrogen, 17a (4mL, 0.11mmol) and acetic anhydride (2.5mL, 0.03mmol) were mixed, and the temperature was raised to 60°C and stirred for 1 hour. After cooling the reaction liquid, a crude product of 17b (6.5 mL) was obtained, and the yield was 100%.

References:

CN112279853, 2021, A Location in patent:Paragraph 0252-0253; 0254-0255

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