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136260-85-0

FURAN-2-YL(THIOPHEN-3-YL)METHANOL synthesis

1synthesis methods
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Yield:136260-85-0 86.6%

Reaction Conditions:

Stage #1: furanwith n-butyllithium in tetrahydrofuran;hexane at -78 - 0;Inert atmosphere;
Stage #2: 3-thiophene carboxaldehyde in tetrahydrofuran;hexane at -78 - 0;Inert atmosphere;
Stage #3: with water;ammonium chloride in tetrahydrofuran;hexane at 0;Inert atmosphere;

References:

Singh, Vishwakarma;Singh, Vikrant [Synthetic Communications,2010,vol. 40,# 9,p. 1280 - 1291] Location in patent:experimental part