Furo[2,3-c]pyridin-3-ol, 2,3-dihydro- (9CI) synthesis

5synthesis methods

Product Name:Furo[2,3-c]pyridin-3-ol, 2,3-dihydro- (9CI)
CAS Number:106531-53-7
Molecular formula:C7H7NO2
Molecular Weight:137.14

10128-71-9
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$8.00/1g

Furo[2,3-c]pyridin-3-ol, 2,3-dihydro- (9CI)

106531-53-7
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Yield:-

Steps:

Multi-step reaction with 5 steps
1: 83 percent / 98percent H₂SO₄ / benzene / 48 h / Heating
2: 62 percent / K₂CO₃ anhydr. / acetone / 2 h / Heating
3: 74 percent / Na / toluene; ethanol / 6 h / Heating
4: 10percent HCl / 2.5 h / Heating
5: 76 percent / sodium borohydride / methanol / 0.5 h / Ambient temperature

References:

Morita, Hiroyuki;Shiotani, Shunsaku [Journal of Heterocyclic Chemistry,1986,vol. 23,p. 549 - 552]

FURO[2,3-C]PYRIDIN-3(2H)-ONE HYDROCHLORIDE

106531-51-5
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106531-53-7
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References

ethyl 3-(2-ethoxy-2-oxoethoxy)isonicotinate

18343-02-7
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$352.00/250mg

106531-53-7
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References

ETHYL 3-HYDROXYFURO[2,3-C]PYRIDINE-2-CARBOXYLATE

106531-50-4
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106531-53-7
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References

3-Hydroxypyridine-4-carboxylic acid ethyl ester

18342-97-7
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References