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151266-48-7

H-3,5-DIIODO-TYR-OME HCL synthesis

1synthesis methods
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Yield:151266-48-7 98%

Reaction Conditions:

Stage #1: methanolwith thionyl chloride at 0; for 0.166667 h;Inert atmosphere;
Stage #2: 3,5-diiodo-l-tyrosine at 20; for 16 h;

References:

Rajput, Sunnia;McLean, Kirsty J.;Poddar, Harshwardhan;Selvam, Irwin R.;Nagalingam, Gayathri;Triccas, James A.;Levy, Colin W.;Munro, Andrew W.;Hutton, Craig A. [Journal of Medicinal Chemistry,2019,vol. 62,# 21,p. 9792 - 9805] Location in patent:supporting information

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