HEXAHYDRO-1H-AZEPINE-3-METHANOL synthesis
- Product Name:HEXAHYDRO-1H-AZEPINE-3-METHANOL
- CAS Number:61472-23-9
- Molecular formula:C7H15NO
- Molecular Weight:129.2
105-60-2
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Yield:-
Steps:
Multi-step reaction with 4 steps
1.1: sodium hydride / tetrahydrofuran / 0.5 h / -5 - 0 °C
1.2: 16 h / 16 °C
2.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere
2.2: 2 h / -78 - 16 °C
3.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / -10 - 0 °C
4.1: palladium(II) hydroxide; hydrogen / methanol / 16 h / 12 °C / 775.74 Torr
References:
US2015/197493,2015,A1
33241-96-2
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