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ChemicalBook CAS DataBase List HEXENAL

HEXENAL synthesis

13synthesis methods
-

Yield:25166-87-4 93%

Reaction Conditions:

with oxalyl dichloride;dimethyl sulfoxide;triethylamine in dichloromethane;1.) -78 deg C, 30 min, 2.) -30 deg C, 1 h;

References:

Aebi, Johannes D.;Deyo, Donald T.;Sun, Chong Qing;Guillaume, Dominique;Dunlap, Brian;Rich, Daniel H. [Journal of Medicinal Chemistry,1990,vol. 33,# 3,p. 999 - 1009]