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ChemicalBook CAS DataBase List hexyl nonan-1-oate

hexyl nonan-1-oate synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / N,N-dimethyl-formamide / 20 °C
1.2: 1 h / 0 °C
1.3: 15 h / 20 °C
2.1: cesium fluoride / acetonitrile / 15 h / 100 °C / Sealed tube

References:

Wu, Hongxiang;Guo, Weijie;Daniel, Stelck;Li, Yue;Liu, Chao;Zeng, Zhuo [Chemistry - A European Journal,2018,vol. 24,# 14,p. 3444 - 3447]