ChemicalBook CAS DataBase List hydroxymethyldiphenylsilane

hydroxymethyldiphenylsilane synthesis

13synthesis methods

Product Name:hydroxymethyldiphenylsilane
CAS Number:778-25-6
Molecular formula:C13H14OSi
Molecular Weight:214.34

1825-59-8 Synthesis

1825-59-8
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778-25-6
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Yield:778-25-6 100 %Chromat.

Reaction Conditions:

with water in acetonitrile at 25; for 0.333333 h;Time;

Steps:

18; 66 (Example 1)

General procedure: Methyldi (methoxy) (phenyl)silane (MePhSi (OMe) 2) 0.5 mmol, Heavy water 10 mmol, Zeolite CBV780 (manufactured by Zeolite) 1 mg, A mixture of 0.9 mL of acetonitrile was placed in the reaction tube and placed in a reaction tube. The mixture was stirred at 25 ° C. (room temperature) for 10 minutes. The product is a nuclear magnetic resonance spectrum measuring device (NMR), Gas chromatograph (GC), And as a result of analyzing with a gas chromatograph mass spectrometer (GC-MS) and measuring the yield of the product by NMR, the result It was found that methyl (phenyl) silanediol-d2 (MePhSi (OD) 2) was produced in a yield of 90% (see Table 1-1).

References:

JP2021/116261,2021,A Location in patent:Paragraph 0053-0054; 0057; 0073-0074

776-76-1 Synthesis