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ChemicalBook CAS DataBase List IBOTENIC ACID MONOHYDRATE

IBOTENIC ACID MONOHYDRATE synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 70 percent / 1.) sodium hydride, 2.) butyl nitrite / tetrahydrofuran / 0.08 h / 0 °C
2: 1.) H2, HCl, 2.) Et3N / 1.) palladium on carbon / 1.) ethanol, 1.5 h 2.) water, 45 min

References:

Madsen, Ulf;Brehm, Lotte;Krogsgaard-Larsen, Povl [Journal of the Chemical Society. Perkin transactions I,1988,p. 359 - 364]

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