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ChemicalBook CAS DataBase List INDAN-2-YL-METHYLAMINE HYDROCHLORIDE

INDAN-2-YL-METHYLAMINE HYDROCHLORIDE synthesis

8synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: N-ethyl-N,N-diisopropylamine; 1,1,1,3,3,3-hexamethyl-disilazane; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide / 0.5 h / 20 °C
2: lithium aluminium tetrahydride / tetrahydrofuran / 7 h / 20 °C / Inert atmosphere; Cooling with ice

References:

THE REGENTS OF THE UNIVERSITY OF MICHIGAN US2012/252807, 2012, A1

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