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Indane-5-carbonitrile synthesis

6synthesis methods
-

Yield:83101-14-8 15% ,69975-67-3 0.26 mmol ,51980-05-3 0.24 mmol ,5737-31-5 0.06 mmol

Reaction Conditions:

Stage #1: terephthalonitrilewith ammonia;sodium at -33;
Stage #2: 1,3-dibromo-propanewith ammonia at -33;Further stages. Further byproducts.;

References:

Panteleeva;Lukyanova;Pokrovsky;Shteingarts [Russian Chemical Bulletin,2007,vol. 56,# 6,p. 1110 - 1118]