IODINEAZIDE synthesis
1synthesis methods
- Product Name:IODINEAZIDE
- CAS Number:14696-82-3
- Molecular formula:
- Molecular Weight:0
Yield:-
Reaction Conditions:
in diethyl etherfreshly prepared, moist AgN3 covered with water cooled to 0°C; addn. of soln. of I2 in ether cooled to 0°C under shaking;; decanting etheric layer at low temp. very fast through dry folder filter into flask with calcined Na2SO4; drying 5 min.; evapn. of ether with dry air until pptn., then in desiccator; washing with small amt. of petroleum ether; (drying); impurity: I2;;
References:
Hantzsch, A.;Schuemann, M. [Chemische Berichte,1900,vol. 33,p. 524 - 524]