IODODIFLUOROACETYL FLUORIDE synthesis
- Product Name:IODODIFLUOROACETYL FLUORIDE
- CAS Number:44507-93-9
- Molecular formula:C2F3IO
- Molecular Weight:223.92
77570-00-4
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44507-93-9
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Yield:44507-93-9 91%
Reaction Conditions:
with cesium fluoride at 90; for 3 h;
Steps:
1 [0091] Synthesis of ICF2C(0)F
[0092] ICF2C(0)F was produced from ICF2CF2OSO2F (350 g, 1.1 mol) in the presence of CsF (15 g, 0.1 mol) and was heated up to 90 °C for 3 hours. ICF2C(0)F was collected in 91 % yield (224 g, 1.0 mol; b.p. 39 to 41 °C).
References:
WO2016/89617,2016,A1 Location in patent:Paragraph 0091-0092
91731-70-3
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44507-93-9
24 suppliers
$45.00/250mg